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KMID : 0380620100420060664
Korean Journal of Food Science and Technology
2010 Volume.42 No. 6 p.664 ~ p.675
Monitoring of Residual Pesticides in Agricultural Products by LC/MS/MS
Kim Mi-Ok

Hwang Hye-Shin
Lim Moo-Song
Hong Jee-Eun
Kim Soon-Sun
Do Jung-Ah
Choi Dong-Mi
Cho Dae-Hyun
Abstract
This survey was carried out to estimate pesticide residue levels in commercial agricultural products in the year 2009. Residues were examined in 16 commodities (rice, foxtail millet, buckwheat, kidney beans, peanuts, sesame, oranges, grapefruit, kiwifruit, spinach, perilla leaves, leeks, garlic stem, garlic, ginger, and oak mushroom) collected from 22 provinces in Korea. Analyses were performed by multi-methods capable of detecting up to 60 pesticides by LC/MS/MS. A total of 510 samples were collected and analyzed. Of the samples, 96.1% contained no detectable pesticide residues. Detectable residues at or below the MRLs were found in 3.5% of the samples. However, in 0.4% of the samples (spinach and leeks), residue (ethaboxam and fluquinconazole) levels exceeded the MRLs. Furthermore, intake assessments of 7 kinds of pesticide residues were carried out, excluding those exceeding the MRLs. The results showed that the ratios of EDI (estimated daily intake) to ADI (acceptable daily intake) were 0.0001-0.0006%, which indicates that the detected pesticide residues were in a safe range. It is concluded that residual pesticides in agricultural products are properly controlled in Korea.
KEYWORD
pesticide, monitoring, agricultural product, LC/MS/MS
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